By Aaron Wold, John K. Ruff
The volumes during this carrying on with sequence supply a compilation of present thoughts and ideas in inorganic man made chemistry. contains inorganic polymer syntheses and practise of significant inorganic solids, syntheses utilized in the improvement of pharmacologically energetic inorganic compounds, small-molecule coordination complexes, and similar compounds. additionally includes priceless details on transition organometallic compounds together with species with metal-metal cluster molecules. All syntheses awarded the following were verified.
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Extra resources for Inorganic Syntheses, Volume 14
Aluminum Trihydrklediethyl Etherate 47 References 1. E. W. Lawless,Inorg. , 9,2796 (1970). 2. D. T. Sauer and J. M. Shreeve, Chem. , 1970,1679. 3. D. Sauer and J. M. , 1, 1 (197 1). 4. A. Haas and D. Y. Oh, Chem. , 102, 77 (1969). ]. 5. A. R. Brandt, H. J. Emelius, and R. N. Haszeldine,]. Chem. Soc.. 1952,2198. 6. E. W. Lawless and L. D. Harman,]. Inorg. Nucl. , 31, 1542 (1969). 10. 3(C2H5)20]+ 3LiCI Submitted by D. L. SCHMIDT,*C. B. ROBERTS,* and P. F. REIGLER* O w k e d by M. F. ,? and E. P. 3 [ (C,H5 )2 01 ,$ have been published,'S2 but the absence of complete experimental details makes duplication difficult.
Bond, and H. I. Schlesinger, J. Am. Chem. , 69, 1199 (1947). 2. E. Wiberg and M. Schmidt, 2. , 66, 333 (1951). 3. E. Wiberg and R. Uson, Rev. Acad. Cienc. , Fis. Quim. Nat. Zaragoza.. 10(2), 35 (1955). 4. D. L. Schmidt and R. S. patent 3,462,288 (1969). 5. W. W. Wendlant and R. Dunham, Anal. Chim. Acta, 19,505 (1958). 1 1 . TRIMETHYLAMMONIUM TETRAPHENYLBORATE (A Rendy Source of Triphenylborone' ) - 4LiC6H5 + BCl3-ether LiB(C, H5 )4 + (CH3) 3 NHCl LiB(C6H5)4+ ether + 3LiCl (CH3 )3 NHB(C6H5 )4 + LiCl Submitted by K.
J. Emelius, and R. N. Haszeldine,]. Chem. Soc.. 1952,2198. 6. E. W. Lawless and L. D. Harman,]. Inorg. Nucl. , 31, 1542 (1969). 10. 3(C2H5)20]+ 3LiCI Submitted by D. L. SCHMIDT,*C. B. ROBERTS,* and P. F. REIGLER* O w k e d by M. F. ,? and E. P. 3 [ (C,H5 )2 01 ,$ have been published,'S2 but the absence of complete experimental details makes duplication difficult. ' Problems inherent in previous methods, such as premature precipitation, decomposition of the alane, and lithium chloride contamination, are avoided.
Inorganic Syntheses, Volume 14 by Aaron Wold, John K. Ruff